AQA · GCSE · Chemistry

    Course version: 8462 · Version from Sept 2018

    Required practical 2: (chemistry only) determination of the reacting…

    Full specification wording

    Titrations (chemistry only): Required practical 2: (chemistry only) determination of the reacting volumes of solutions of a strong acid and a strong alkali by titration.

    In this required practical you find the volume of one solution that exactly reacts with a known volume of another.

    Checked against the AQA 8462 specification (opens in a new tab) on .

    • Point 2 of 2
    • 3 key terms

    Study notes

    From the checked teaching notes for this specification point.

    The idea

    In this required practical you find the volume of one solution that exactly reacts with a known volume of another. A strong acid, such as hydrochloric acid, is placed in a burette and a measured volume of strong alkali, such as sodium hydroxide solution, is pipetted into a conical flask with a few drops of indicator. You record the initial burette reading, then add acid steadily while swirling, slowing near the end point as the indicator colour changes. Repeating until concordant titres agree improves reliability. You must use accurate procedural techniques, such as rinsing the burette with the acid and reading the bottom of the meniscus at eye level, to ensure precise volume measurements.

    What earns the marks

    • Records initial and final burette readings to two decimal places and calculates each titre by subtraction.
    • Uses a pipette and filler to deliver an accurate fixed volume of alkali into a clean conical flask.
    • Adds indicator in small amounts and swirls the flask during the titration to mix the solutions.
    • Repeats the titration until concordant titres are obtained and uses a mean of concordant values.
    • Applies accurate procedural techniques, such as reading the meniscus at eye level, to ensure precise measurements.

    Common mistakes and how to put them right

    • Reading the top of the meniscus instead of the bottom.

      Put it right by aligning eye level with the bottom of the curved surface.

    • Forgetting to record the initial burette reading.

      Put it right by noting it before adding any acid.

    • Using the first rough titre in the mean.

      Put it right by repeating and averaging only concordant accurate titres.

    Exam tips

    • State the colour change at the end point for the indicator used, for example phenolphthalein changing from pink to colourless when acid is added to alkali.
    • Ensure you subtract the initial volume from the final volume to find the titre.
    • Give burette readings to two decimal places and quote the mean titre with the same precision.

    Try the lesson

    The start of the Titrations (chemistry only): Required practical 2: (chemistry only) determination of the reacting volumes of solutions of a strong acid and a strong alkali by titration. lesson, made from checked teaching notes for this specification point.

    Have a go first

    In the titration practical, which piece of apparatus is used to add the alkali to the acid a little at a time near the end point?

    Listen

    In this required practical you find the volume of one solution that exactly reacts with a known volume of another. A strong acid, such as hydrochloric acid, is placed in a burette and a measured volume of strong alkali, such as sodium hydroxide solution, is pipetted into a conical flask with a few drops of indicator. You record the initial burette reading, then add acid steadily while swirling, slowing near the end point as the indicator colour changes. Repeating until concordant titres agree improves reliability. You must use accurate procedural techniques, such as rinsing the burette with the acid and reading the bottom of the meniscus at eye level, to ensure precise volume measurements. A strong answer earns marks for these points. Records initial and final burette readings to two decimal places and calculates each titre by subtraction. Uses a pipette and filler to deliver an accurate fixed volume of alkali into a clean conical flask. Adds indicator in small amounts and swirls the flask during the titration to mix the solutions. Repeats the titration until concordant titres are obtained and uses a mean of concordant values. A common slip: Reading the top of the meniscus instead of the bottom. Instead, aligning eye level with the bottom of the curved surface. Exam tip: State the colour change at the end point for the indicator used, for example phenolphthalein changing from pink to colourless when acid is added to alkali.

    See it

    A top-to-bottom flowchart with nine steps. First, strong acid is placed in a burette. Second, a fixed volume of strong alkali is pipetted into a conical flask. Third, a few drops of indicator are added. Fourth, the initial burette reading is recorded. Fifth, acid is added steadily while swirling. Sixth, the addition is slowed near the end point as the indicator colour changes. Seventh, the final burette reading is recorded and the titre calculated. Eighth, the titration is repeated until concordant titres agree. Ninth, the mean of concordant values is used.
    The sequence of steps in the titration required practical, from setting up the acid and alkali through to using a mean of concordant titres.

    Key words

    Say what each word means before you turn the card.

    Accurate measurement of volume

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    Concordant results and reliability

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    Procedural techniques for precision

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    See every definition
    Accurate measurement of volume
    Using accurate procedural techniques, such as rinsing the burette with the acid and reading the bottom of the meniscus at eye level, to ensure precise volume measurements.
    Concordant results and reliability
    Repeating the titration until concordant titres agree, which improves reliability, and using a mean of concordant values.
    Procedural techniques for precision
    Accurate procedural techniques, such as rinsing the burette with the acid and reading the bottom of the meniscus at eye level, to ensure precise measurements.

    Label the diagram

    Some boxes have lost their names. Pick the right name for each number.

    The diagram again, with 3 boxes numbered instead of named. A top-to-bottom flowchart with nine steps. First, strong acid is placed in a burette. Second, a fixed volume of strong alkali is pipetted into a conical flask. Third, a few drops of indicator are added. Fourth, the initial burette reading is recorded. Fifth, acid is added steadily while swirling. Sixth, the addition is slowed near the end point as the indicator colour changes. Seventh, the final burette reading is recorded and the titre calculated. Eighth, the titration is repeated until concordant titres agree. Ninth, the mean of concordant values is used.
    • 1Box 1

    • 2Box 2

    • 3Box 3

    0 of 3 labelled

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